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800px; left: 100px; top: 62px;z-index:2;"><div class="yibuFrameContent tem_1_4 newsItemTitleBind_Style1 " style="overflow:visible;;" ><h1 class="w-title">聚合氯化鋁的生產方法和生產工藝過程</h1></div></div><div id="smv_tem_2_28" ctype="newsItemCrumbsBind" class="smartRecpt esmartMargin smartAbs " cpid="1133604" cstyle="Style1" ccolor="Item0" areaId="" isContainer="False" pvid="" tareaId="" re-direction="x" daxis="All" isdeletable="True" style="min-height: 35px; width: 400px; left: 87px; top: 25px;z-index:3;"><div class="yibuFrameContent tem_2_28 newsItemCrumbsBind_Style1 " style="overflow:visible;;" > <div class="w-crumbs"> <a href="/" class="w-crumbs-item">首頁</a> <span class="w-crumbs-category "> </span><i class="w-arrowicon mw-iconfont w-crumbs-category ">ꄲ</i> <span class="w-crumbs-category "> </span><a href="/NewsInfoCategory?categoryId=79946,79946" class="w-crumbs-item w-crumbs-category ">聚合氯化鋁</a> <span class="w-crumbs-caption "> </span><i class="w-arrowicon mw-iconfont w-crumbs-caption">ꄲ</i> <span class="w-crumbs-caption"> </span><span class="w-crumbs-caption">聚合氯化鋁的生產方法和生產工藝過程</span> </div>  <script type="text/javascript"> $(function () { $('#smv_tem_2_28').smartNPCrumbsControl({ controlId: 'smv_tem_2_28', languageId:2,isHideTitle:true }); }); </script></div></div><div id="smv_tem_3_50" ctype="newsItemContentBind" class="smartRecpt esmartMargin smartAbs " cpid="1133604" cstyle="Style1" ccolor="Item0" areaId="" isContainer="False" pvid="" tareaId="" re-direction="all" daxis="All" isdeletable="True" style="min-height: 126px; width: 850px; left: 75px; top: 165px;z-index:4;"><div class="yibuFrameContent tem_3_50 newsItemContentBind_Style1 " style="overflow:visible;;" ><style> .w-detail ul, .w-detail li, .w-detail ol { list-style: inherit; } .w-detail ul, .w-detail ol { padding-left: 40px; } </style>  <div id="tem_3_50_txt" class="w-detailcontent"> <div class="w-detail"><p><span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> </span></span></span></span><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"><a href="http://www.zacatecaswebnews.com/" target="_blank" title="聚合氯化鋁"><span style="color:#000000"><strong>聚合氯化鋁</strong></span></a></span></span></span><span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun">的生產方法有鋁礬土生產聚合氯化鋁、金屬鋁生產聚合氯化鋁、氫氧化鋁生產聚合氯化鋁等多種多種方法工藝，淄博枘澎環?？萍脊静捎玫木酆下然X生產配方是先進的鋁礬土法生產工藝配方，生產過程對工業廢棄物循環利用，生產成本大大降低，并且生產的聚合氯化鋁產量高、含量高、質量好。<br /> <img alt="gg" height="156" src="https://nwzimg.wezhan.cn/contents/sitefiles2035/10175980/images/4793500.png" width="419" /> <br /> <br /> 鋁礬土生產聚合氯化鋁生產方法、工藝過程： <br /> 以鋁土礦為原料制備聚合氯化鋁的生產方法較復雜，由于這些礦物中的鋁一般不能直接被酸溶出，必須經過一系列加工處理之后才能呢個使鋁溶出。按鋁的溶出方式可分為酸法和堿法。酸法適用于粘土礦、煤矸石、高嶺土、一水軟鋁石、三水鋁石等礦物原料。<br /> 聚合氯化鋁生產配方：鋁礬土加鋁酸鈣粉。鋁礬土是鋁硅酸鹽類礦物，按結構含水狀況分為三水鋁石（Al<sub>2</sub>O<sub>3</sub>·3H<sub>2</sub>O），一水軟鋁石（γ-Al<sub>2</sub>O<sub>3</sub>·H<sub>2</sub>O）和一水硬鋁石（α-Al<sub>2</sub>O<sub>3</sub>·H<sub>2</sub>O），提取鋁的難度一次遞增。</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 我國三水鋁石的富礦較少，生產混凝劑的鋁礬土原料多為一水軟鋁石，工藝流程是以一水軟鋁石為原料，將礦石粉碎磨細后在沸騰爐中以650-800℃焙燒，把熟礦粉在反應罐中加溫加壓溶出鋁液，溶出時可采用不足量酸分段溶出，可加入氫氟酸提高溶出率，然后在以鋁酸鈣提高鹽基度；分段溶出時灌內溫度為120-130℃，壓力為2.0-2.2㎏/㎝<sup>2</sup>,Al<sub>2</sub>O<sub>3</sub>的溶出率為90%以上。</span></span></span></span></p> <p><span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 聚合氯化鋁生產工藝流程圖1：</span></span></span></span></p> <p><span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> <img alt="圖1鋁礬土生產聚合氯化鋁工藝" height="119" src="http://www.ggmyjs.com/uploadfile/201710/6/1138355597.jpg" width="382" /></span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 此方法生產的聚合氯化鋁鹽基度在60%-90%，氧化鋁質量分數為25%-31%，該方法溶解時間短，溶出率高，但是沒有在常壓下生產的產量高。</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 也可以利用鋁礬土生產鋁酸鈣后，直接用鹽酸和鋁酸鈣一步法生產聚合氯化鋁的工藝。用高品位鋁礬土與石灰石經破碎、烘干、球磨、制坯、煅燒、粉磨后，生產出Al<sub>2</sub>O<sub>3</sub>含量較高且Al<sub>2</sub>O<sub>3</sub>活性較強的鋁酸鈣粉，可直接用于生產聚合氯化鋁等凈水劑，然后用鹽酸處理該鋁酸鈣，獲得相應的鋁鹽。在該溶出過程中，鋁酸鈣中其他雜志，如Ca、Si、Fe、Ti、Mg等也會部分溶出，在控制鹽酸用量的前提下，反映過程中可直接獲取堿式氯化鋁，并伴有堿式氯化鐵生成。聚合氯化鋁的生產方法反應式為：</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> CaO·Al<sub>2</sub>O<sub>3</sub>+3HCl=Al<sub>2</sub>(OH)<sub>n</sub>Cl<sub>6-n</sub>+CaCl<sub>2</sub>+2H<sub>2</sub>O</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 當溶出反應進展到一定程度，且PH值較為適當的時候，堿式氯化鋁相鄰兩個羥基就會發生架橋作用而聚合和或自聚，并最終轉化為聚合氯化鋁。對應的反應式如下：</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> mAl<sub>2</sub>(OH)<sub>n</sub>Cl<sub>6-n</sub>=[Al<sub>2</sub>(OH)<sub>n</sub>Cl<sub>6-n</sub>]m</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 另外，一水硬鋁石（α-Al<sub>2</sub>O<sub>3</sub>·H<sub>2</sub>O）或其它含鋁礦物難溶于酸，可采用堿法制備聚合氯化鋁；用碳酸鈉、石灰制得鋁酸鈉，再分解制得凝膠氫氧化鋁，用凝膠法制得聚合氯化鋁。</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 聚合氯化鋁生產工藝流程圖2：</span></span></span></span></p> <p><span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> <img alt="圖2鋁礬土生產聚合氯化鋁工藝" height="141" src="http://www.ggmyjs.com/uploadfile/201710/6/1139188941.jpg" width="402" /></span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 對粒度的要求為100μm者占95%以上，焙燒溫度以860℃為宜，偏差不能超過±10℃。若溫度太低，氧化鋁以γ-Al<sub>2</sub>O<sub>3</sub>的形存在，可溶于堿，不能達到化學選礦的要求；溫度過高，則會生成多鋁紅柱石，從而損失氧化鋁。加堿溶出時需要260-280℃的高溫，這時鋁以鋁酸鈉的形式進入溶液。為得到凝膠氫氧化鋁，應向鋁酸鈉溶液中通入二氧化碳，加入鹽酸，使凝膠氫氧化鋁溶解，升溫聚合便可制的液態聚合氯化鋁。<br /> <img alt="聚合氯化鋁生產設備" height="225" src="https://nwzimg.wezhan.cn/contents/sitefiles2035/10175980/images/4342977.png" width="363" /></span></span></span></span></p> <p><span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"><strong> </strong>金屬鋁法生產聚合氯化鋁</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 金屬鋁法所用原料主要是鋁加工的下腳料鋁屑、鋁灰和鋁渣等。工藝上可分為酸法、堿法、中和法三種。目前，我國以金屬鋁為原料生產PAC的廠家大多采用酸法生產。酸法具有反應速度快。設備投資少、工藝簡單、操作方便的優點，但溶液中的雜質含量偏高，產品質量不穩定，設備腐蝕嚴重。堿法生產工藝則難度較高，設備投資較大，成本較高，其應用受到一定限制。中和法的特點是綜合了酸法和堿法兩者的優點。酸溶法生產聚合氯化鋁的的主要反應式為：</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 2Al+6H<sup>+</sup>=2AL<sup>3+</sup>+3H<sub>2</sub></span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 2Al<sup>3+</sup>+nH<sub>2</sub>O=AL<sub>2</sub>(OH)<sub>n</sub><sup>(6-n)+</sup>+nH<sup>+</sup></span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> m[AL<sub>2</sub>(OH)<sub>n</sub><sup>(6-n)+</sup>]=[AL<sub>2</sub>(OH)<sub>n</sub>]m<sup>m(6-n)+</sup></span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 此法原料來源極為有限，生產過程會產生大量氫氣和熱量，氫氣連同氯化氫、水蒸汽、粉塵等四處彌漫，控制不當有引起爆炸的危險，故操作環境惡劣,安全性較差，常見于一些小規模露天生產、手工操作的企業。</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 近年來，有些廠家研究開發了利用廢鋁箔包裝材料生產聚合氯化鋁的新技術。該技術既能充分回收利用其中的鋁，又可回收利用其中的紙、塑料，具有一定的經濟效益和良好的社會效益。</span></span></span></span><br /> </p> <p><span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"><strong> </strong>氫氧化鋁酸溶法生產聚合氯化鋁</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 氫氧化鋁酸溶法是以氫氧化鋁為原料，國內和國外都普遍采用的一種工藝。氫氧化鋁純度高，生產的產品重金屬含量很低，但由于氫氧化鋁酸溶性比較差，因此一般在反應釜中采用加溫加壓的方法溶出鋁液，經分離熟化后即可得到聚合氯化鋁產品，還可以在反應釜中加壓加熱，這樣可以使氫氧化鋁中鋁的溶出率達到90%以上。這種工藝相對比較簡單，但是所得產品的鹽基度偏低，在40%左右，基本反應式為：</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> Al(OH)<sub>3</sub>+HCl=Al(OH)<sub>2</sub>Cl+H<sub>2</sub>O</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> Al(OH)<sub>2</sub>Cl+HCl=Al<sub>2</sub>(OH)<sub>3</sub>Cl<sub>3</sub>+H2O</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> Al<sub>2</sub>(OH)<sub>3</sub>Cl<sub>3</sub>→[Al<sub>2</sub>(OH)<sub>n</sub>Cl<sub>6-n</sub>]m（m＜10）</span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 為提高產品的鹽基度，逐漸發展到第二步，為了不引入其它重金屬雜質，一般采用在低鹽基度產品中加入鋁屑和鋁酸鈉。這樣鹽基度一般可提高到70%以上。<br /> 氫氧化鋁酸溶法生產聚合氯化鋁工藝流程圖：</span></span></span></span></p> <p> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"><img alt="圖4氫氧化鋁兩步法生產聚合氯化鋁工藝流程圖" height="146" src="http://www.ggmyjs.com/uploadfile/201710/6/1140477381.jpg" width="408" /></span></span></span></span><br /> <span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"> 在采用鋁酸鈣粉調整鹽基度時，可以將鹽基度調的更低，這樣可以加強氫氧化鋁的溶解，減少不溶性氫氧化鋁的量。鹽酸的濃度可以控制在20%以上，酸的濃度越大，氫氧化鋁的溶解性越好。在實際生產中，反應配料比為Al(OH)<sub>3</sub>∶鋁酸鈣礦粉=（0.6-0.9）∶1（質量比）。在常壓下、于80-100℃反應3-4h，過濾即得液體產品，通過噴霧烘干或者滾筒烘干即可得到固體產品。</span></span></span></span><br /> <span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"><span style="color:#777777"> </span></span></span></span><span style="color:#777777"><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun">氫氧化鋁酸溶法生產聚合氯化鋁的工藝</span></span></span></span><span style="line-height:2"><span style="font-size:14px"><span style="font-family:SimSun"><span style="color:#777777">關鍵是碳酸化分解，分解過程中若條件控制不當，制得凝膠氫氧化鋁在鹽酸中溶解性不好，或即使溶解，產品的穩定性也不好，分解反應也可利用碳酸氫鈉代替二氧化碳。此工藝的優點是生產條件溫和，聚合氯化鋁質量好，缺點是流程長，生產成本較高。<br /> <br /> <img alt="枘澎500手機" height="196" src="https://nwzimg.wezhan.cn/contents/sitefiles2024/10122542/images/4556465.png" width="391" /><br /> 枘澎環?？萍脊驹?/span><a href="http://www.zacatecaswebnews.com/" target="_blank" title="聚合氯化鋁"><span style="color:#000000"><strong>聚合氯化鋁</strong></span></a><span style="color:#777777">及聚氯化鋁、聚丙烯酰胺、聚合氯化鐵等凈水劑領域研發生產、應用服務領域已有三十多年的專業沉淀積累，可全方位為市政生活水處理、工業水處理及生產企業廢水處理提供優質產品、創新設計及調試、運營服務。 </span></span></span></span></p> </div> </div>  <script type="text/javascript"> $(function () { var contentWidth = parseInt($('#smv_tem_3_50').css("width")); ///長圖自適應屏幕 $('#smv_tem_3_50 table').each(function () { $(this).removeAttr("width"); if ($(this).width() > contentWidth) { $(this).css("width", "100%"); } }); var splitLength = $('#tem_3_50_txt').find("div").html().split("_ueditor_page_break_tag_"); if (splitLength.length > 1) { 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